Thursday 12 October 2017

ACID BASE TITRATION USING PRIDE OF BARBADOS FLOWER (Caesalpinia pulcherrima) EXTRACT AS AN INDICATOR




ABSTRACT
Samples of Pride of Barbados flower were extracted and analysed for its indicator properties in acid-base titration. Acetone, ethanol and acetone/ethanol mixtures were used for the extraction. The results of the indicator extracts showed greenish to amber colour in basic medium and pink at the end point for all the extracts. The results of statistical analysis were compared with that of the standard indicator (phenolphthalein) for precision. Extracts X showed calculated FR value (1.0) < the critical FR value (6.3) for (P = 0.05) and calculated Td (0.4) < critical Td (1.27) for (p = 0.05). Extract Y gave calculated FR (2.0) < critical FR (6.3) and calculated Td (0.2) < critical Td (1.27) and extract Z gave calculated FR (1.0) < critical FR (6.3) and calculated Td (1.0) < critical Td (1.27) respectively. In all, the results showed that there is no significant difference between the extracts X, Y, Z and the standard indicator (phenolphthalein). Therefore, it is recommended that Pride of Barbados flower extract should be used for standardization in acid base titration.